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Preparation And Photocatalytic Properties Study Of Magnetism Fe3O4/SnO2/TiO2

Posted on:2006-04-30Degree:MasterType:Thesis
Country:ChinaCandidate:T BaiFull Text:PDF
GTID:2121360182475907Subject:Applied Chemistry
Abstract/Summary:PDF Full Text Request
In this paper, the magnetism core Fe3O4 have been prepared with Fe(NO3)3 and(NH2)2·H2O. Then Fe3O4/SnO2 have been prepared through precipitation method,and in this reaction the SnCl4·nH2O is the main material, the Fe3O4 is themagnetism core. At last Fe3O4/SnO2/TiO2 coated particles have been prepared withTi(OC4H9)4 and Fe3O4/SnO2 as precursors by Sol-Gel method. In order to improvethe photocatalytic degradation activity of Fe3O4/SnO2/TiO2 for methylic orange, theconditions of preparing were selected and the better photocatalytic activity werereceived. The dynamic of methylic orange photocatalytic degradation reaction andeffect of H2O2 were investigated. It's morphology and structure were characterizedby IR, XRD, TEM, XPS and VEM. The result indicated: the photocatalytic activityof Fe3O4/SnO2/TiO2 are better than those TiO2 and Fe3O4/ TiO2, It's photocatalyticactivity are just a little worse than SnO2/TiO2. H2O2 are useful for improving thephotocatalytic activity of Fe3O4/SnO2/TiO2 and the reaction is zero order reaction.The sample Fe3O4/SnO2/TiO2 have good magnetism and its easy to reclaim...
Keywords/Search Tags:magnetism, Sol-Gel method, Fe3O4/SnO2/TiO2, photocatalytic degradation methylic orange
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