Sensing Characteristic Of One-dimensional ZnO Nanostructures | Posted on:2007-10-02 | Degree:Doctor | Type:Dissertation | Country:China | Candidate:X H Wang | Full Text:PDF | GTID:1101360185962395 | Subject:Radio Physics | Abstract/Summary: | PDF Full Text Request | In this paper, one dimensional ZnO nanostructure was studied as sensor material by quartz crystal microbalance(QCM). The results of these studies were listed below:1. Preparation and characterization of one-dimensional ZnO nanostructure and doped ZnO nanostructure was studied in this paper. The ZnO nanotetrapods were synthesized by evaporating highly pure zinc pellets (99.999%) at 900℃ in air and then distributed onto the electrode surfaces of the quartz crystal at room temperature. The synthesized ZnO nanotetrapods were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The ZnO nanotetrapods were synthesized by evaporating highly pure zinc pellets (99.999%) at 900℃ in air and PdCl2 was doped on by traditional solution mixing process. Then the mixed solution distributed onto the electrode surfaces of the quartz crystal at room temperature. Pd2+ doped ZnO nanotetrapods were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM)2. ZnO nanotetrapods were prepared and studied for the humidity detection application. The humidity sensors developed were featured by combination of a quartz crystal as a transducer and ZnO nanotetrapods as a sensing element. The experimental results indicated that the response of the sensors varied with the thickness of the ZnO nanotetrapods layer. The maximum frequency sensitivity was nearly 100Hz/%RH (relative humidity) in the humidity range of 40% to 80%RH (relative humidity). The ZnO nanotetrapods sensors also had a good frequency stability and reproducibility. Thus it was found that ZnO nanotetrapods were a potential humidity sensing material.3. Pd2+ doped ZnO nanotetrapods were prepared and studied for the humidity detection application. The humidity sensors developed were featured by combination of a quartz crystal as a transducer and Pd2+ doped ZnO nanotetrapods as a sensing element. The experimental results indicated that the response of the sensors varied with the different dosage PdCl2. Linear regression algorithm was...
| Keywords/Search Tags: | quartz crystal microbalance, one-dimensional ZnO nanostructure, ZnO nanowire, ZnO nanotetrapods, humidity sensor, relative humidity, ammonia sensor, Pd, doping, biosensor, uricase, uric acid, immobilization, wireless sensor network, node | PDF Full Text Request | Related items |
| |
|