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Development of a quadrupole ion trap mass spectromete

Posted on:2001-09-26Degree:Ph.DType:Dissertation
University:The University of Texas at DallasCandidate:Hebert, Joseph EllisFull Text:PDF
GTID:1461390014960575Subject:Atomic physics
Abstract/Summary:
Because of its potential to be made portable the quadrupole ion trap (QPIT) is a prime candidate for specialized applications such as atmospheric studies, other field measurements, or measurements anywhere a laboratory instrument would be prohibitively inconvenient. To utilize the QPIT in such ways it is necessary to design and construct custom built instruments. A QPIT mass spectrometer was constructed as the foundation for such future development. Two ionization schemes were employed. Direct electron bombardment was used for in situ ion production, and UV photoionization was used to produce ions external to the trap. Calibration measurements determined that the system performed as theory dictated. It was also demonstrated that the system was capable of sampling the atmosphere and detecting the presence of an atmospheric contaminant. Finally, DC bias foils were invented as a novel approach to mass isolation in the trap. The use of DC bias foils was demonstrated to be an exceptionally easy and inexpensive method of controlling the contents of the QPIT.
Keywords/Search Tags:Ion, QPIT, Trap, Mass
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