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Research On Three-dimensional Oriented Porous Chitosan Scaffolds

Posted on:2011-05-03Degree:MasterType:Thesis
Country:ChinaCandidate:Y Z LiFull Text:PDF
GTID:2154360302986060Subject:Polymer engineering
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(1) Chitosan scaffolds were prepared by in-situ precipitation. Scanning electron microscope (SEM) were used to study features of the scaffolds and the results reveal that the scaffolds are three-dimensional oriented. The porosity was above 88% and compressive strength was as high as 1.80MPa.(2) Chitosan (CS) /hydroxyapatite (HA) composite scaffolds were prepared by in-situ precipitation. HA was synthesised around the chitosan molecularchain. IR and XRD proved the exitance of HA. SEM photos showed that the needle-like HA particles evenly spreaded in the chitosan bulk. The porosity was around 91.2% and compressive strength was as high as 0.267MPa..(3) Chitosan/Ferriferrous oxide (Fe3O4) composite scaffolds were prepared by in-situ precipitation and modified by mineralization and aging procedure. IR and XRD proved the exitance of Fe3O4 and the obvious effect of chemical bond between the magnetic particles and chitosan moleculars. The digital photographs showed that the scaffold with Fe3O4 has more obvious layered structure. SEM proved that column-shape magnetic particals spreaded in the chitosan bulks. The porosity was up to 95% and compressive strength was as high as 0.668MPa.
Keywords/Search Tags:In-situ precipitation, chitosan, three-dimensional oriented, hydroxyapatite, ferriferrous oxide
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