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Multicomponent Systems Carve Divorced Terpinene Distillation Column

Posted on:2002-01-01Degree:MasterType:Thesis
Country:ChinaCandidate:C M YuanFull Text:PDF
GTID:2191360032451369Subject:Applied Chemistry
Abstract/Summary:PDF Full Text Request
The selected catalysate of teipaie by solid acid is a multi-componat and heat saisitive mataials. It is pol)merized by heat .The polyma take much tmuble to our distillaiiai We sepa-ate the tmi-component Into two amponals: the light and the hea拁.y. We use equilibrium method to obtain their saturated vapour uressure at diffa~nt au ilative volatility and FLJGmethod to estimate the distillation plates of Sluzer Gauze packing to obtain teapinolene(90w%). By the way, we use the same method and multi-conipcuent distillation to obtain the distillation plates. The two plates and the documait are showing no difl~nce. The distillation plates are about C. Weusethedistihlatkmt]bewlxEeheight is2.lm to research the distillation conditicm,thatare itssureofthetopis aboutA1 -A2ntnHg ;therefluxratioare R1, R2, R3-R4 Those opaation cxmditkx are duplicative. The wail effect is the main niattaibat afl~c1s the distillation efliciaicy. To get the higher distlllatim effect; we use the fluid distribution on the top of the packing But the afict is much smalL...
Keywords/Search Tags:heat saisitive mataials, vaconm batch distillation, FUGmethod, wall effect, distillation efficiency
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