| In this article, the transparent glass ceramics containing CaMoO4 nanocrystals was successfully prepared by molten-crystallization method. It was found the best formula of the sample after several experiment and adjustment of the main material composition. The XRD test was taken on the samples after heat treatment. We could find the main crystalline phase was CaMoO4 when we compared the XRD curve with the standard card. The optimal heat treatment system of glass matrix can be determined after DSC, XRD, SEM, optical transmittance analysis and many times experiment.Eu3+ doped transparent glass ceramics containing CaMoO4 nanocrystals was successfully prepared in this paper. It was easy to found that the optimal doping amount of Eu3+ was 5%. we can get the optimal heat-treatment system by various test and analysis of Tb3+ doped transparent glass ceramics containing CaMoO4 nanocrystals. The luminescence properties of the sample was best when the doping concentration of Tb3+ was 7.0%, while the doping quenching phenomenon has been discussed. |
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