The Synthesis And Manufacture Of 3-Amino-1H-1,2,4-Triazole | Posted on:2004-04-29 | Degree:Master | Type:Thesis | Country:China | Candidate:X Wang | Full Text:PDF | GTID:2121360125963435 | Subject:Chemical Engineering | Abstract/Summary: | PDF Full Text Request | Synthesis of 3-amino-1-H-1,2,4-triazole from amino guanidine bi-carbonate and formic acid was studied in this paper, the related reaction parameters were optimized, particularly the acylation and cyclisation were intensively examined . Water is employed as solvent in replace of inert organic solvent, then to provide a new economical method for the production of 3-amino-1-H-1,2,4-triazole. The process for the production of 3-amino-1H-1,2,4-triazole is designed on the results of research work. The equipment setting and running tests were accomplished and the high quality products were obtained .
| Keywords/Search Tags: | 3-amino-1H-1,2,4-triazole, Salt formation, Acylation, cyclisation | PDF Full Text Request | Related items |
| |
|