The Valuable Chinese Medicine Of Oviductus Ranae's Quality Evaluate Research (Ⅲ)

Purpose:By producing Oviductus Ranae Jilin and Liaoning, Heilongjiang. Inner Mongolia, Shaanxi, Qinghai, and North Korea to a total of 14 samples of Oviductus Ranae intrinsic quality of research and comparative analysis, as Oviductus Ranae Quality Evaluation System to provide scientific Basis.Methods:①Pharmacopoeia reference and the method of conventional medicine Oviductus Ranae indicators were compared.②Oviductus Ranae by TCL on a comparative study of medicine;and using polyacrylamide gel electrophoresis for 14 samples of Oviductus Ranae and eight kinds of adulterants were compared.③The UV method, GC-MS method,14 samples of Oviductus Ranae total amino acids and fatty acids were determined.④The HPLC method for 14 samples of Oviductus Ranae,8 copies Oviductus Ranae and its adulterants in different parts of China Forest 1-A hydantoin levels were analyzed.Results:①14 copies Oviductus Ranae swelling sample, extract, crude fat content were some differences, but the difference was small; Heavy metal detection, samples comply with pharmacopoeial formulary standard. arsenic salt in detecting, sample G, heilongjiang samples are overweight phenomenon with standard arsenic spot color differ not quite, the rest of the samples comply with pharmacopoeial standards.②14 copies Oviductus Ranae TLC sample spots are basically the same, but the spot is somewhat different color; Jilin Electrophoresis Oviductus Ranae produced no difference in the Korean province of Jilin Oviductus Ranae production capacity were compared Oviductus Ranae Some differences Oviductus Ranae Confused quite different.③14 copies Oviductus Ranae determination of total fatty acid and ammonia are some of their differences.④14 copies Oviductus Ranae sample 1-A hydantoin concentration difference between the larger, samples of which H, Jiaohe and Heilongjiang were relatively less;Preliminary Checklist Mingha Ranae adulterants in different parts of China and also contain Rana 1-A hydantoin.Conclusion:In different regions Ma oil samples 14. both in quality, there is a certain difference;Preliminary determination Ma oil promiscuous product display ha its different parts of rana chensinensis also contains 1-methyl hein.